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← Document results/DEP Box 13/508 X 10/27/01 AN 11/23/01
Document / 7 pages

Pesticide calibration verification results, sample AD25049, Nov 2001

Machine-extracted title · confidence 95%

Calibration verification report showing recovery percentages for standard pesticide compounds in sample AD25049.

NYC-WTC_000009343–000009349

Folder label: “508 X 10/27/01 AN 11/23/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Signal #1 : C:\HPCHEM\1\DATA\508F\011121\4TOXC1.D\ECD1A.CH Vial: 22 Signal #2 : C:\HPCHEM\1\DATA\508F\011121\4TOXC1.D\ECD2B.CH Acq On : 25 Nov 2001 10:40 am Operator: Nefliu Sample : tox icl Inst : 104 Mise : Multiplr: 1.00 IntFile Signal #1: events.e IntFile Signal #2: events2.e Quant Time: Nov 26 13:31 2001 Quant Results File: 011116T.RES Quant Method : C:\HPCHEM\1\METHODS\011116T.M (Chemstation Integrator) Title : 508 CHLORINATED PESTICIDES TOXAPHENE7/28/99 Last Update : Fri Nov 09 16:13:01 2001 Response via : Initial Calibration DataAcq Meth : 508F2.M Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info : Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 6) S 2,4-DDD SURROGAT 0.00 0.00 0 0 N.D. d N.D. d Spiked Amount 0.200 Recovery 0.00% 0.00% Target Compounds 1) TOXAPHENE PEAK 1 35.05 35.00 31186 27683 0.795m 0.651m 2) TOXAPHENE PEAK 2 39.05 36.50 105917 68481 0.872m 0.639m# 3) TOXAPHENE PEAK 3 40.51 38.44 67526 48748 0.665m 0.661 4) TOXAPHENE PEAK 4 45.35 39.52 65087 52126 0.604m 0.547 5) TOXAPHENE PEAK 5 45.89 40.55 53251 45052 0.422m 0.709m#

0-

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 4TOXC1.D 011116T.M Mon Nov 26 15:05:31 2001 Page 1

NYC-WTC_000009348

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NYC-WTC_000009348Source: NYC Law Department, mirrored locally

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