Method 508 sample log sheet, Oct-Nov 2001

2 Quantitation Report 2 - - o O 2 Signal #1 Signal #2 : C:\HPCHEM\1\DATA\508\112401\25831.D\ECDlA.CH Vial: 47 : C:\HPCHEM\1\DATA\508\112401\25831.D\ECD2B.CH CD — o U 1 O Acq On : 25 Nov 2001 7:46 pm Operator: Nefliu C O Sample : sample Inst : 105 O O O o' O Mise : Multiplr: 1.00 "0 00 o co o IntFile Signal #1: EVENTS.E IntFile Signal #2: EVENTS.E — Quant Time: Dec 4 15:59 2001 Quant Results File: 120401P.RES 0 O o Q C Quant Method : C:\HPCHEM\1\METHODS\508\120401P.M (Chemstation Integrator) 3 Title : 508 Chlorinated Pesticides CD

Last Update : Tue Dec 04 15:25:58 2001 Response via : Multiple Level Calibration DataAcq Meth : PESTPCB.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info : 25831.D\ECD1A w 4

CM 100000

80000

60000

40000 W W 8 5 & 8

20000 7 । | 20 । । । । | g । । | । । । । [ । 88 4JH r kill । i i i i । । I । । । । । i । । । । । । । [ [ । । ।—r Time 0.00 2.00 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 Response 25831. D\ECD2B

S 8000

6000

S C o R 4000 W— & CM y8 5 5 %,3, 2000 $,8,36 1 I I L Time 0.00____ 2.00 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 25831.D 120401P.M Tue Dec 04 15:59:29 2001 Page 2