DEP Method 508 sample log, Oct-Nov 2001

2 Quantitation Report 2 - - o o 3 Data File Acq On : C:\HPCHEM\1\DATA\508\112101\25495.D\ECD1A.CH Vial: : 23 Nov 20101 10:38 pm Operator: 57 Nefliu CD — o "0 1 o Sample : sample Inst : 105 C o O o Mise Multiplr: 1.00 o' o : EVENTS.E o IntFile "0 o o) — 0 CD Data File C:\HPCHEM\1\DATA\508\112101\25495.D\ECD2B.CH vial : 57 o Acq On 23 Nov 101 10:38 pm Operator: Nefliu o Q C Sample sample Inst : 105 3 CD Misc Multiplr: 1.00 IntFile EVENTS.E Quant Time Nov 28 11:26 19101 Quant Results File: 112601P.RES

Quant Method : C:\HPCHEM\1\METHODS\508\112601P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Wed Nov 28 11:18:57 2001 Response via : Multiple Level Calibration DataAcq Meth : PESTPCB.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info : Response 25495.D\ECD1A 100000

80000

60000 < 40000 A------_2 V-----d a 28 Q Oeg 20000 ................................. &........ £ I I5 1 [ Dil I I I I I I I ] I I 1 I [l I I I----- 1—T—I I ■' l fu, . Time 0.00 2.00 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 Response _ 25495.D\ECD2B 8000-

6000 A 4000 ___A-------------—A — 1g | S o g 2000 E 92° ' 1 1 ■ i 1 1 ■ ■ i 1 ...................................................................... I ?............... 38: 1 ' 1 1 1 1 1 1 1 1 1 1 | 1 ‘ 1 1 | 1 1 1 1 | 1 1 1 1 I ‘ 1 । । | । । _______________ ।—।—।—।—।—।—।—।—,—।—1—।—।—,—।—।—।—,—,—।—1—i—i—1—।—- r me 0.00 2.00 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00

25495.D 112601P.M Wed Nov 28 11:26:37 2001 Page 2