DEP Method 508 sample log, Oct-Nov 2001

Quantitation Report 2 2 - K o o 2 Data File Acq On : C:\HPCHEM\1\DATA\508\112101\25460.D\ECD1A.CH vial: 53 : 23 Nov 20101 8:08 pm Operator: Nefliu CD — o Sample : sample Inst : 105 "0 I C o O o o Mise Multiplr: 1.00 o' o IntFile : EVENTS.E "0 o o CH — 0 CD Data File C:\HPCHEM\1\DATA\508\112101\25460.D\ECD2B.CH Vial: 53 O Acq On 23 Nov 101 8:08 pm Operator: Nefliu o Q C Sample sample Inst : 105 3 C Mise Multiplr: 1.00 IntFile EVENTS.E Quant Time Nov 28 11:23 19101 Quant Results File: 112601P.RES

Quant Method : C:\HPCHEM\1\METHODS\508\112601P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Wed Nov 28 11:18:57 2001 Response via : Multiple Level Calibration DataAcq Meth : PESTPCB.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info : Response 25460.D\ECD1A 150000

100000

50000

0— W WUlus 1&s .............. —Yg8k _!_ 8_— K A

mm 0.00 2.00 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 ■ esponSe 25460.D\ECD2B |

10000

5000 k Us I_a LA——-— ___________ ________ ________ _________________________ 1 6 888 ------------- . ................................................................................................ ....................... ‘ f 1 ' i ‘ | « ’ 28 kl | « 13 l ' ’ । । | । । i । | i i i i । i—i—i—i—।—i—। ।—i—]—r 0.00 2.00 4.00 6.00 8.00 10.00 12.00 J4.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00

25460.D 112601P.M Wed Nov 28 11:23:24 2001 Page 2