NYC 9/11 Public Portal Document
Method 508 OC Checklist Batch 15420 / "1)0/
1. Calibration: /IC J %RSD within20% F Unext. LCS within 20% of T.V. F
3 levels --
CCV )alternating 2 stds, each within 20% of T.V. P
—. One at beginning of sequence, and one at end
2. Extraction within 14 days of collection: N Injection within 30 days of extraction: N
3. LPC standard: S/N F PGF (PJ F Res
4. Endrin and DDT breakdown: Within 20% prior to calibration or verification:
5. Surrogate recoveries: List samples that failed and were reextracted.
6. Method blank: F
7. Field blank: ( Not needed ) P F
8. LCS per batch: Failures present Yes( No ;
9. Matrix spike every 10 samples: Failures present Yes ) No
or per batch
10. Duplicate matrix spike: Failures present (Yes No
with each matrix spike
11. Quarterly Check sample within 30% of limits Not needed Failures present Yes No
12. Duplicate samples: List positive samples which were reanalyzed:
13. Problems were encountered: Yes No What type:
Batch sheet Injection Log Manual
Analyst _ Supv. Decision Approved
Rev. 11/8/01
i)
N YC-WTC_000006601
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