Initial GCMS analysis report for sample AE01940 conducted by analyst DLV on March 13, 2002.
NYC-WTC_000006362–000006370Folder label: “GCMS X 2/15/02 A 2/9/02 & 2/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document • LL1-
Data File : C:\HPCHEM\l\DATA\FEB1502\1940.D Vial: 14 Acq On : 16 Feb 2002 4:04 am Operator: 209 GALOS Sample : re-extract Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 8 15:39 2002 <Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.34 152 552101 20.00 ug/1 -0.02 10) Naphthalene-d8 15.98 136 2136945 20.00 ug/1 -0.02 17) Acenaphthene-diO 21.30 164 1128122 20.00 ug/1 -0.02 29) Phenanthrene-diO 25.74 188 1574274 20.00 ug/1 -0.03 38) Chrysene-dl2 33.81 240 1000035 20.00 ug/1 -0.04 44) Perylene-dl2 38.10 264 669330 20.00 ug/1 -0.03
System Monitoring Compounds 37) 2,4-DDD 30.82 235 60447 3.68 ug/mL 0.32 Spiked Amount 5.000 Recovery = 73.60%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.03 128 182 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.75 149 307 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 1940.D GCMS0208.M Fri Mar 08 16:05:19 2002 Page 1
NYC-WTC_000006364
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NYC-WTC_000006377
Quality control page documenting surrogate compound recovery rates for a gas chromatography mass spectrometry run.
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Gas chromatography-mass spectrometry analysis of environmental sample AD31344 conducted on February 15, 2002.
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Gas chromatography-mass spectrometry analysis of environmental sample AD31136 conducted on February 15, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006393
Quality control page documenting surrogate compound recovery rates for a gas chromatography mass spectrometry run.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005877
Analytical report showing surrogate recovery data for sample AE00164 analyzed on February 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005651
Laboratory report for DEP sample AE02968 showing unknown compounds and surrogate recovery data from February 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005868
Analytical report showing surrogate recovery data for sample AE00162 analyzed on February 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
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Gas chromatography-mass spectrometry analysis of environmental sample AE02971 conducted on February 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005660
Laboratory report for DEP sample AE02969 showing unknown compounds and surrogate recovery data from February 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005716
Gas chromatography-mass spectrometry analysis of sample AE03015 conducted on 2/15/2002, detecting 2,4-DDD and other unknown compounds with specified detection limits.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052736
GC/MS analysis report for sample AE01037 showing surrogate recovery data generated on February 26, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052726
GC/MS analysis report for sample AE01036 showing surrogate recovery data generated on February 26, 2002.
1 shared topics · similarity 0.995
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Initial GCMS analysis report for sample AE01940 conducted by analyst DLV on March 13, 2002.
Filed in the same folder
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Quality control page documenting surrogate compound recovery rates for a gas chromatography mass spectrometry run.
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Calibration table listing retention times and responses for deuterated standards including naphthalene-d8.
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