GCMS analysis results for sample AE03248, March 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03248.D Vial: 3 . Acq On : 1 Mar 2002 5:39 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.611 17 21 25 rBV 31562 54656 0.38% 0.068% 2 3.916 45 48 53 rBV 15612 27944 0.19% 0.035% 3 4.638 103 112 125 rVB4 13275 61329 0.42% 0.076% 4 4.864 129 132 143 rW3 22589 77725 0.54% 0.097% 5 5.011 143 145 151 rW 23666 43056 0.30% 0.054%

6 5.891 221 223 243 rBV 970328 2203377 15.21% 2.740% 7 9.707 557 561 567 rBV 4804810 9275407 64.04% 11.536% 8 9.876 573 576 583 rBV3 10268 28360 0.20% 0.035% 9 12.541 807 812 815 rW 91867 166546 1.15% 0.207% 10 13.195 865 870 875 rBV 6732017 13379959 92.37% 16.641%

11 13.376 883 886 891 rVB 13576 29900 0.21% 0.037% 12 13.590 901 905 913 rBV3 10491 31873 0.22% 0.040% 13 16.548 1163 1167 1169 rW 15218 26940 0.19% 0.034% 14 18.332 1319 1325 1331 rBV 6834680 14112581 97.43% 17.552% 15 22.283 1669 1675 1683 rW 43734 90534 0.63% 0.113%

16 22.633 1701 1706 1711 rBV2 6634735 14484694 100.00% 18.015% 17 27.724 2151 2157 2161 rBV 1047561 1977289 13.65% 2.459% 18 30.490 2395 2402 2407 rBV 5452346 13054859 90.13% 16.236% 19 31.088 2451 2455 2461 rW4 18171 49941 0.34% 0.062% 20 34.407 2743 2749 2783 rBV 4167562 11228182 77.52% 13.965%

Sum of corrected areas: 80405152

3248.D HP022102.M Mon Mar 04 12:33:27 2002 Page 1

NYC-WTC_000006150