GCMS analysis results for sample AE03245, March 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03245.D Vial: 6 • Acq On : 1 Mar 2002 2:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 2-Butenal, 2-methyl- $$ Cro... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 3.99 0.07 ug/L 32287 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butenal, 2-methyl- $$ Crotonal... 84 C5H80 001115-11-3 9 2 Formamide, N-(cyanomethyl)- 84 C3H4N2O 005018-27-9 9 3 Cyclopentanone 84 C5H80 000120-92-3 9 4 2-Butenal, 2-methyl- (CAS) $$ 2-... 84 C5H80 001115-11-3 9 Abundance Scan 55 (3.995 min): 03245.D (-) m/z 83.95 100.00% 84 55

5000 41 • 44 51 . 3.60 3.80 4.00 4.20 4.40 Of - - I 1 1 1 ' I ' ' m/z 55.10 80.29% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #3217:2-Butenal, 2-methyl- $$ Crotonaldehyde, 2-methyl- $... 55 84 29

5000 _AA 3.60 m/z 3.80 4.00 41.10 4.20 4.40 30.38% 26 37 44 51 । m/z-> O+ —PP 20 25 - 30 35 40 45 50 55 +.. 69. P 60 65 70 75 80 1"" I" 85 90 Abundance #3103: Formamide, N-(cyanomethyl)-

1, Ajii A' MA 29

3.60 3.80 1 1 ■ 4.00 —AA— 4.20 4.40 84 55 m/z 53.10 13.82% 5000

40 36 45 , 66 u ol ■ ■ i' ■1 ■ । ■1 - - 1.. . miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #3268: Cyclopentanone 3.60 3.80 4.00 4.20 4.40 m/z 83.10 13.02%

5000 41 84 27

m/z-> 0 38 1' i1111111111 ' 1111 1 ■ ■ i1 20 25 30 35 40 45 50 -H 50 1 r 11 ‘ 55 ■ i'1111'1 11111111 11 60 65 70 75 80 I-... 85 90 L 3.60 IIII**III*I*’[** 3.80 4.00 4.20 4.40

)3245.D HP022102.M Mon Mar 04 12:33:05 2002 Page 5

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