DEP document page with method and sample data, March 2002

NYC 9/11 Public Portal Document

DFTPP

Data File : C:\MSDCHEM\1\5973N\02MAR01\0301DF.D Vial: 1 Acq On : 1 Mar 2002 8:25 am Operator: Sample : dftpp Inst : Instrume Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method

Abundance TIC: 0301 DF.D

8000000

6000000

4000000

2000000-

0 L, — Time-> 22.50 23.00 23.50 24.00 24.50 25.00 25.50 26.00 Abundance Scan 1838 (24.122 min): 0301 DF.D 198 442 600000

400000 77 127 51 255

110 200000 275 224 93 | OTTTPT + 149H+HH 1141—+181 — H 4239 + , ;. 1 . . 226 . . 323.346 365 383.403 423 Krr I I । । r । ii 1 i । i i ii 17 । । | r rt“i । ii r i |1 ‘ । i ("I j i i "I । TI m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440

Spectrum Information: Scan 1838

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 30 60 50.3 341632 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 43.3 294080 PASS 70 69 0.00 2 0.6 1715 PASS 127 198 40 60 54.4 369280 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 678656 PASS 199 198 5 9 6.9 46960 PASS 275 198 10 30 22.2 150912 PASS 365 198 1 99 2.6 17936 PASS 441 443 1 99 73.9 90128 PASS 442 198 40 110 90.1 611584 PASS 443 442 17 23 19.9 121968 PASS

0301DF.D HP022102.M Fri Mar 01 09:56:49 2002

NYC-WTC_000006012