GCMS analysis results for sample AE03074, March 2002

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Data File C:\MSDCHEM\l\DATA\022802\03074 .D Vial: 8 - Acq On 1 Mar 2002 6:07 pm Operator: McLean Sample 2/12/02 GC SCAN Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Octanal, 7-methoxy-3,7-dime... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.60 1.64 ug/L 549397 1,4-Dichlorobenzene-d4 9.58

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octanal, 7-methoxy-3,7-dimethyl- . . . 186 C11H22O2 003613-30-7 9 2 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 3 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 9 4 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 Abundance Scan 278 (5.597 min): 03074.D (-) m/z 73.10 100.00% 73 8000

6000

4000 F’’ TT1‘t 2000 45 5.20 5.40 5.60 5.80 6.00

m/z-> .. 155.a 1 1 1 r 1 1 1 1 11 .. . 1 1 T 20 40 60 80 87 103 100 120 140 160 m/z 45.10 14.81%

Abundance #95640: Octanal, 7-methoxy-3,7-dimethyI- $$ Methoxycitrone... 73 8000

6000

4000

2000 V _ 1_ 5.20 5.40 5.60 5.80 6.00 m/z 71.10 7.61% 20 41 55 15 29H 1 1 ....... . 85 95 111121 137 153 171 -i '| । 11 ' i '' ' ' ' i ' ' ' ' i' ' ' ' ' i ' ' ' ' i ' ' '' ' i m/z-> 20 40 60 80 100 120 140 160 Abundance #9665: 3-Pentanol, 3-methyl- 73 8000 ‘I ■ ■ 1 1 1 5.20 5.40 5.60 5.80 6.00 6000 m/z 55.10 4.89% 4000 55 2000; 43 87 29 ■ ■ i ■ ' ■ ■ I ‘ ll ' i ■ ■ ■ ■ i ■ ■ ■ ■ i 1 ' ' ' i ' ' ' ' i ' ' ' ' i m/z—> 20 40 60 80 100 120 140 160 Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... A*...... 73 । 1 1 ■ 1 । ■ 1 5.20 5.40 5.60 5.80 6.00 8000 m/z 69.10 4.73%

6000

4000 43 55 87 2000;

m/z—> , 4— 20 29

40 — 60 ■ i ' 1 ' ' i ' ' ' ' i ■ ' ' 1 i ■ ' ' ' i ' ' ' ' i 80 100 120 140 160 ................ 5.20 5.40 5.60 5.80 6.00

03074.D 5080202.M Mon Mar 04 05:52:44 2002 Page 3

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