Laboratory report for DEP sample AE03014 showing unknown compounds and surrogate recovery data from February 15, 2002.
NYC-WTC_000005698–000005706Folder label: “GCMS X 2/7/02 A 2/9/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\l\DATA\FEB0802\3014.D Vial: 38 Acq On 9 Feb 2002 9:15 pm Operator: 209 GALOS Sample GC/MS SCAN 2/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 13 10:52 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Feb 08 15:29:22 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.35 152 488836 20.00 ug/1 0.00 10) Naphthalene-d8 15.99 136 1900938 20.00 ug/1 0.00 17) Acenaphthene-diO 21.31 164 1041499 20.00 ug/1 0.00 29) Phenanthrene-diO 25.76 188 1535080 20.00 ug/1 0.00 38) Chrysene-dl2 33.83 240 1087987 20.00 ug/1 -0.01 44) Perylene-dl2 38.12 264 719275 20.00 ug/1 0.00
System Monitoring Compounds 37) 2,4-DDD 30.83 235 74440 3.90 ug/mL 0.33 Spiked Amount 5.000 Recovery = 78.00%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21 -oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.05 128 496 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.78 149 2478 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 3014.D GCMS0208.M Wed Feb 13 10:53:37 2002 Page 1
NYC-WTC_000005700
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NYC-WTC_000005716
Gas chromatography-mass spectrometry analysis of sample AE03015 conducted on 2/15/2002, detecting 2,4-DDD and other unknown compounds with specified detection limits.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005660
Laboratory report for DEP sample AE02969 showing unknown compounds and surrogate recovery data from February 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005725
Gas chromatography-mass spectrometry analysis of environmental sample AE02971 conducted on February 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005651
Laboratory report for DEP sample AE02968 showing unknown compounds and surrogate recovery data from February 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005679
Laboratory report for DEP sample AE02972 showing unknown compounds and surrogate recovery data from February 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005689
Laboratory report for DEP sample AE02973 showing unknown compounds and surrogate recovery data from February 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005642
Laboratory report for DEP sample AE02967 showing unknown compounds and surrogate recovery data from February 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005763
Gas chromatography-mass spectrometry analysis of environmental sample AD31662 conducted on February 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009721
Analytical results page for sample AE01220 processed on February 25, 2002, showing surrogate recovery data.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016575
Laboratory report for DEP sample AD31464 identifying unknown compounds and surrogate recovery results from February 15, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018353
Laboratory report documenting GCMS analysis of sample AD31457 conducted on February 13, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009477
Gas chromatography mass spectrometry results for sample AE00897 analyzed on February 26, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000005604
Department of Environmental Protection GCMS sample tracking record for the World Trade Center site dated February 2002.
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NYC-WTC_000005605
Fragmented header page from a Method 508 laboratory document dated February 7-9, 2002, showing instrument parameters.
Filed in the same folder
NYC-WTC_000005607
Instrument sequence log listing sample IDs and analytical runs processed on February 8, 2002, including calibration checks.
Filed in the same folder
NYC-WTC_000005610
Laboratory report for DEP sample AE02966 listing concentrations of target compounds including nitrosamines and chlorobenzenes.
Filed in the same folder
NYC-WTC_000005614
Reference analysis report for DEP sample AE02966 showing measured values for target compounds against detection limits.
Filed in the same folder