GCMS DFTPP calibration report, Feb 5 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02FEB05\00003A.D Vial: 2 Acq On 5 Feb 2002 3:46 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.488 5 10 13 rVB 37614 56485 0.24% 0.043% 2 3.613 19 21 25 rBV 50563 80697 0.34% 0.062% 3 3.922 45 48 53 rBV 26953 42288 0.18% 0.032% 4 4.230 73 75 79 rBV 253103 421269 1.76% 0.323% 5 5.920 221 223 229 rBV 89241 188979 0.79% 0.145%

6 9.539 537 540 545 rBV 41330 94711 0.40% 0.073% 7 9.630 545 548 551 rW 45862 101248 0.42% 0.078% 8 9.710 551 555 561 rW 7447219 15089685 63.02% 11.574% 9 9.836 561 566 579 rW 61640 218603 0.91% 0.168% 10 13.204 855 861 865 rBV 9827405 21220807 88.62% 16.277%

11 13.375 873 876 883 rVB 29127 57830 0.24% 0.044% 12 16.549 1149 1154 1157 rBV 31403 59892 0.25% 0.046% 13 18.341 1305 1311 1317 rBV 9817883 22479326 93.88% 17.242% 14 22.280 1651 1656 1661 rBV2 107994 206220 0.86% 0.158% 15 22.645 1681 1688 1693 rBV2 9531925 23944767 100.00% 18.366%

16 22.771 1697 1699 1717 rVB 153417 437426 1.83% 0.336% 17 27.726 2127 2133 2139 rBV 1315299 2294477 9.58% 1.760% 18 29.678 2299 2304 2317 rBV 15609 51671 0.22% 0.040% 19 30.512 2369 2377 2421 rBV 8213604 23474680 98.04% 18.006% 20 34.428 2713 2720 2761 rBV2 6409734 19851795 82.91% 15.227%

Sum of corrected areas: 130372856

00003A.D SCAN508.M Thu Feb 21 10:18:49 2002 Page 1

NYC-WTC_000004804