GCMS DFTPP calibration report, Feb 5 2002

Machine-extracted title · confidence 95%

Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB05\30648A.D Vial: 5 Acq On 5 Feb 2002 2:03 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 2-Propanol, 1-(2-methoxy-l-... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 9.63 0.18 ug/L 135838 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 2-Propanol, 1-(2-methoxy-l-methy. . . 148 C7H16O3 020324-32-7 83 2 DIPROPYLENEGLYCOL METHYL ETHER $... 148 C7H16O3 020324-32-7 72 3 TRIPROPYLENE GLYCOL 2 192 C9H20O4 000000-00-0 56 4 BIS(1-METHYL-2-HYDROXYETHYL)ETHER 134 C6H1403 000000-00-0 50 Abundance Scan 548 (9.630 min): 30648A.D (-) m/z 59.10 100.00% 50

5000 45 103 73 I 1 1 1 1 I 1 1 1 I 1 1 1 1 T1 1 1111 r 11111111, J,hi । II"' 11,11 84 9.20 9.40 9.60 9.80 10.00 । TT’’1’’11112*1*1’0100’30T’T m/ z 45.10 44.44% 0 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #43943:2-Propanol, 1-(2-methoxy-1 -methylethoxy)- $$ Dipro... 50

5000

I. 45 103 9.20 9.40 9.60 9.80 10.00 73 31 m/z 103.05 43.46% 130 0- i । 11 ITrI 11 ’ 11 । I Ji 11 —I 11 । । i1 1111 > ■ i > >111 'H1' ।"1 11—2000001——— nfz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #43944: DIPROPYLENEGLYCOL METHYL ETHER $$ 2-Propanol, 1-(2... 50 103 i ■ ■ ■ 1 I ' ' 9.20 9.40 9.60 9.80 10.00 5000 m/z 73.10 31.68% 45 73 31

0 —P15PP 130 ■ ■ i " ■ ■ i ■" ■ I ■1 ■ ■ i' ■111 ■'1 ■ ।1 ■1 ■ । m/z—> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 #102327: TRIPROPYLENE GLYCOL 2 50 _WA 9.20 9.40 9.60 9.80 10.00 m/z 41,. 10 20.66%

5000

45 103

0 -mm 1101111172, 89 TTT I"117 130 1'........ I" 161 I-*sh’sss’’’’m T-p-r TTT I A । ■ ■ ’ I’ ' n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 9.20 9.40 9.60 9.80 10.00

30648A.D SCAN508.M Thu Feb 21 10:19:05 2002 Page 9

NYC-WTC_000004926

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