GCMS DFTPP calibration report, Feb 5 2002

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02FEB05\30648A.D Vial: 5 Acq On 5 Feb 2002 2:03 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first- max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.613 17 21 29 rBV2 58218 99273 0.40% 0.075% 2 3.922 43 48 53 rVB 30818 53456 0.22% 0.040% 3 4.241 71 76 81 rBV 243883 412344 1.67% 0.312% 4 5.920 219 223 235 rBV 93263 204490 0.83% 0.155% 5 7.187 331 334 355 rVB 78753 189149 0.77% 0.143% 6 ’ 9.539 537 540 545 rBV 52457 125234 0.51% 0.095% 7 9.630 545 548 551 rW 59170 135838 0.55% 0.103% 8 9.710 551 555 561 rW 7959007 15137059 61.37% 11.440% 9 9.836 561 566 579 rW 65482 223199 0.90% 0.169% 10 13.192 855 860 865 rBV 9810494 21607572 87.61% 16.330%

11 13.375 873 876 883 rVB 27180 57676 0.23% 0.044% 12 16.549 1151 1154 1157 rBV 32677 54751 0.22% 0.041% 13 18.341 1305 1311 1317 rBV 10116757 23384143 94.81% 17.672% 14 22.280 1651 1656 1661 rBV 114331 207156 0.84% 0.157% 15 22.645 1681 1688 1693 rBV2 9675857 24663502 100.00% 18.639%

16 22.771 1697 1699 1713 rVB 153310 385447 1.56% 0.291% 17 27.726 2127 2133 2139 rW 1382369 2454569 9.95% 1.855% 18 29.690 2299 2305 2317 rVB2 12445 44325 0.18% 0.033% 19 30.512 2369 2377 2381 rBV 8353608 23048450 93.45% 17.419% 20 34.428 2713 2720 2757 rBV 6588057 19833363 80.42% 14.989%

Sum of corrected areas: 132320996

30648A.D SCAN508.M Thu Feb 21 10:19:03 2002 Page 1

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