GCMS DFTPP calibration report, Feb 5 2002

Machine-extracted title · confidence 95%

Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report * Data File : C:\MSDCHEM\1\5973N\02FEB05\29232A.D Vial: 4 Acq On 5 Feb 2002 1:13 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- $$ ... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 3.50 0.09 ug/L 65046 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 86 2 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 83 3 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 72 4 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 53 Abundance Scan 11 (3.499 min): 29232A.D (-) m/z 74.00 100.00% 74 82 5000 47 M.. 35 3.50 3.60 3.70 3.80 3.90 11!iIIj11111111 i 1111 mmmTTT m/ z 82.00 50.02% 0 — TTTTTT 1’11111/1’1’1111’1 m/z—> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 74

5000 82 3.50 3.60 3.70 3.80 3.90 ' ' 47 m/z76.00 32.09% 35 0 HHH . ... । 109 m/z—> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 -rrr-p- — 1111 “ ।1 ‘" i" “ i11" ।।"

Abundance

5000

.. 0 ll. ‘ 38 #11643: Dichloroacetonitrile $$ Acetonitrile, dichloro-

11 47

1 95 102 108 "Thr . .................. r “' i" " i" " i ‘ " i ■' 74 82 3' ‘ ' 1 ' ' ' ' I ' ' ' ' I 1 1 1 1 I 1 1 1 Trl ‘ 1 I 3.50 3.60 3.70 3.80 3.90

m/z-> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 Abundance #11644: Acetonitrile, dichloro- 74 3.50 3.60 3.70 3.80 3.90 111 35 m/z 47.00 24.17% 5000 82

47 40

mfe-> 0 11’ 1+444 -rai + 100 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 TTTp- ■ i1 ■" ।" " i" " i" " i" " i11 ■' i1" AAAAA 3.50 3.60 3.70 3.80 3.90

29232A.D SCAN508.M Fri Feb 22 11:44:17 2002 Page 3

NYC-WTC_000004882

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