DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004494–000004704

Folder label: “GCMS X 1/30/02 A 2/26/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB26\02084 .D Vial: 1 Acq On : 26 Feb 2002 2 :44 pm Operator: Sample : 508 scan Inst Instrumen Mise : February 26, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 9 1,3,4-Thiadiazol-2-amine Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 12.87 0.08 ug/L 53082 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3,4-Thiadiazol-2-amine 101 C2H3N3S 004005-51-0 7 2 Isopropyl isothiocyanate $$ Prop... 101 C4H7NS 002253-73-8 4 3 3H-l,2,4-Triazole-3-thione, 1,2-... 101 C2H3N3S 003179-31-5 4 4 CH3CH2CH(CH3)ONO $$ sec-Butyl ni... 103 C4H9NO2 000924-43-6 4 Abundance Scan 841 (12.868 min): 02084.D (-) m/z 43.10 100.00% 43 101

5000 73 .......... A ’ I’T in 59 12.60 12.80 13.00 13.20 0- n T[— rr । j < ■ । । । । । । ■ । । + m 7 ' । | IT ' r 11' i'111 r ■1 ■ i ‘ ■ i "I“" I" m/ Z 101.00 97.78% mfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #8737:1,3,4-Thiadiazol-2-amine 101 74

5000 45 12.60 12.80 13.00 13.20 60 m/z 73.00 34.98%

m/z—> 0 m + 11" I m I I I I | I I I I | ! I i1" ' i " " r '1' i " " i " " i l l-r | | i । 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 ।

Abundance #8799: Isopropyl isothiocyanate $$ Propane, 2-isothiocyanato- 43 101 AM 12.60 12.80 13.00 13.20 5000 m/ z 45.10 23.10% 60 86 54 70 0 ‘ ।111111'' I''1 111111111 ■ ।1 ■ i" ■11 ■ ■111 "i""i ""i ""i .. . .... I" /z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #8732:3H-1,2,4-TriazoIe-3-thione, 1,2-dihydro- (CAS) $$ 3... 101 12.60 12.80 13.00 13.20 m/ z 41.10 17.81% 5000 42 74 30 60 47 0 i " '' I - TPPT+ i " " i1 " 85 ‘I""I"1‘i""i 1 ■11 ■ ■" i"

mfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 12.60 12.80 13.00 13.20

02084.D HP022102.M Wed Feb 27 08:34:47 2002 Page 11

NYC-WTC_000004599

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999