NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\DEC2701\LBD.D Vial: 38
Acq On : 29 Dec 2001 7:39 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/18 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Jan 24 14:16 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator).
Title : 209 625/TCLP calibration table
Last Update : Tue Jan 22 11:56:23 2002
Response via : Initial Calibration
DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.68 152 1189787 20.00 ug/1 -0.02
10) Naphthalene-d8 15.28 136 4614641 20.00 ug/1 -0.03
17) Acenaphthene-dl0 20.57 164 2294219 20.00 ug/1 -0.01
29) Phenanthrene-dl0 24.98 188 3430841 20.00 ug/1 -0.01
38) Chrysene-dl2 33.02 240 2054348 20.00 ug/1 -0.01
44) Perylene-dl2 37.12 264 1161436 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 30.07 235 132318 3.51 ug/mL 0.00
Spiked Amount 5.000 Recovery = 70.20%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.54 74 2571 N.D.
3) bis(2-Chloroethyl)ether 11.13 93 5338 N.D.
4) 1,3-Dichlorobenzene 11.59 146 4874 N.D.
5) 1,4-Dichlorobenzene 11.73 146 5745 N.D.
6) 1,2-Dichlorobenzene 12.25 146 4833 N.D.
7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 13.07 117 1986 N.D.
11) Nitrobenzene 13.36 77 187 N.D.
12) Isophorone 14.06 82 9094 N.D.
13) bis(2-Chloroethoxy)methane 14.75 93 571 N.D.
14) 1,2,4-Trichlorobenzene 15.19 180 3785 N.D.
15) Naphthalene 15.33 128 15925 N.D.
16) Hexachlorobutadiene 15.89 225 2222 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 18.91 162 7112 N.D.
20) Dimethylphthalate 20.01 163 9360 N.D.
21) 2,6-Dinitrotoluene 20.27 165 708 N.D.
22) Acenaphthylene 20.11 152 8114 N.D.
2 3) Acenaphthene 20.65 153 10079 N.D.
24) 2,4-Dinitrotoluene 21.39 165 198 N.D.
25) Diethylphthalate 22.10 149 12296 N.D.
26) 4-Chlorophenyl-phenylether 22.24 204 4512 N.D.
27) Fluorene 22.19 166 9240 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
LBD.D GCMS1126.M Thu Jan 24 14:17:46 2002 Page 1
NYC-WTC_000004192
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