NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\FEB0802\31464.D Vial: 54
Acq On : 10 Feb 2002 2:41 pm Operator: 209 GALOS
Sample : GC/MS SCAN 2/8 Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Feb 14 16:36 2002 Quant Results File:
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Wed Feb 13 11:43:23 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response/ Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.35 152 41557V 20.00 ug/1 0.00
10) Naphthalene-d8 15.99 136 1610993 20.00 ug/1 0.00
17) Acenaphthene-diO 21.31 164 860635 20.00 ug/1 0.00
29) Phenanthrene-diO 25.75 188 1282500 20.00 ug/1 -0.01
38) Chrysene-dl2 33.82 240 898773 20.00 ug/1 -0.02
44) Perylene-dl2 38.11 264 5/8200 20.00 ug/1 -0.01
System Monitoring Compounds
37) 2,4-DDD 30.83 235 45356 3.52 ug/mL 0.33
Spiked Amount 5.000 Recovery = 70.40%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 /4 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 /93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 14 6 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.0d 146 0 N.D.
7) 2,21 -oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0 $00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 6.00 77 0 N.D.
12) Isophorone /o.oo 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene , 0.00 180 0 N.D.
15) Naphthalene / 16.04 128 251 N.D.
16) Hexachlorobutadiene / 0.00 225 0 N.D.
18) Hexachiorocyclopent adiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene / 0.00 162 0 N.D.
20) Dimethylphthalate / 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene / 0.00 165 0 N.D.
22) Acenaphthylene / 0.00 152 0 N.D.
23) Acenaphthene / 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene / 0.00 165 0 N.D.
25) Diethylphthalate / 22.78 149 448 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene / ' 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
31464.D GCMS0208.M Thu Feb 14 16:37:16 2002 Page 1
NYC-WTC_000004170
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