NYC 9/11 Public Portal Document
Quantitation Report (Not Reviewed)
Data File : C:\HPCHEM\1\DATA\DEC2701\30709.D Vial: 47
Acq On : 30 Dec 2001 4:24 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/18 Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Jan 24 15:05 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Tue Jan 22 11:56:23 2002
Response via : Initial Calibration
DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 1525136 20.00 ug/1 -0.03
10) Naphthalene-d8 15.28 136 5858444 20.00 ug/1 -0.03
17) Acenaphthene-diO 20.56 164 2919114 20.00 ug/1 -0.02
29) Phenanthrene-diO 24.98 188 4410945 20.00 ug/1 0.00
38) Chrysene-dl2 33.03 240 2796315 20.00 ug/1 0.00
44) Perylene-dl2 37.12 264 1658846 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 30.06 235 175805 3.63 ug/mL 0.00
Spiked Amount 5.000 Recovery = 72.60%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.50 74 556 N.D.
3) bis(2-Chloroethyl)ether 11.15 93 2935 N.D.
4) 1,3-Dichlorobenzene 11.59 146 2734 N.D.
5) 1,4-Dichlorobenzene 11.72 146 3576 N.D.
6) 1,2-Dichlorobenzene 12.24 146 2784 N.D.
7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 13.07 117 745 N.D.
11) Nitrobenzene 13.26 77 172 N.D.
12) Isophorone 14.11 82 1254 N.D.
13) bis(2-Chloroethoxy)methane 14.93 93 207 N.D.
14) 1,2,4-Trichlorobenzene 15.18 180 1700 N.D.
15) Naphthalene 15.34 128 10604 N.D.
16) Hexachlorobutadiene 15.90 225 539 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 18.92 162 1610 N.D.
20) Dimethylphthalate 19.99 163 1103 N.D.
21) 2,6-Dinitrotoluene 20.27 165 1125 N.D.
22) Acenaphthylene 20.12 152 1188 N.D.
23) Acenaphthene 20.65 153 1426 N.D.
24) 2,4-Dinitrotoluene 21.28 165 1000 N.D.
25) Diethylphthalate 22.10 149 10223 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 22.20 166 642 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
30709.D GCMS1126.M Thu Jan 24 15:05:17 2002 Page 1
NYC-WTC_000004305
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