GCMS DFTPP calibration verification results, Feb 25, 2002

2 quantltdt1on KepULt - Z O Data File : C:\MSDCHEM\1\DATA\022502\CAL80B.D Vial: 29 - S-I Acq On : 25 Feb 2002 1:01 pm Operator: McLean o co Sample : CAL 80 2/25/02 2ND INJ Inst : Instrumen — 1° Mise o Multiplr: 1.00 O O O MS Integration Params: BENZO.P C O Quant Time: Feb 26 8:28 2002 O Quant Results File: 5080202.RES CT C 00 o' co Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) 0 03 o Title : Quantitation For Method 508gcscan — 0 Last Update : Mon Feb 25 19:17:14 2002 O Response via : Initial Calibration o Abundance o TIC: CAL80B.D C 2 CD 1.1e+07 8 3

8 g € 1e+07 I1 © o § 1 B 86 78 g t sS t1s 2 § S b & €S. 0 aco © 1 & w s 9000000 2 z 78 £ S i 13 £ Is a §

8000000 © o © 89 55 Eg 0 § I I 48 4 se I§ 1 f a [[ 8 s 1 S it ft 8 1 N I S sj g8 fl 525 5 s8 7000000 885 K p $0 85 §1 t 2 > 8 a l , 2 I 6000000 &r rP82 a s x o 5 1 | 3 i 5 I o JC s8Q o 3el 3 S I s I to £

5000000 h: S 5 o ! I h § ! .2

as ®

I 0 3 j ] N ll 4000000 3 13 3000000 i z 2 8 S CQ

I6 k 2000000

1000000

Time—> 0 6.00 8.00 10.00 1 TT TI T —r -r fr 1* — A 1II **Tmr T Vr-T r ---P38.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00

CAL80B.D 5080202.M Wed Feb 27 09:00:43 2002 Page 3