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GCMS analysis results for sample AD31341 with surrogate data, Feb

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Laboratory report for sample AD31341 showing GCMS analysis of unknown compounds and surrogate recovery on February 15, 2002.

NYC-WTC_000003880–000003890

Folder label: “GCMS X 1/28/02 A 2/8/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\FEBO8O2\31341.D Vial: 25 Acq On 9 Feb 2002 8:39 am Operator: 209 GALOS Sample RE-EXTRACT 1/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 13 8:51 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Feb 08 15:29:22 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.76 178 202 N.D. 34) Anthracene 25.76 178 202 N.D. 35) Di-n-butylphthalate 27.71 149 15796 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.82 228 1328 N.D. 42) Bis(2-ethylhexyl)phthalate 34.03 149 450 N.D. 43) Chrysene 33.82 228 1328 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 38.11 252 1499 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 31341.D GCMS0208.M Wed Feb 13 08:52:10 2002 Page 2

NYC-WTC_000003883

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NYC-WTC_000003883Source: NYC Law Department, mirrored locally

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