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Document / 9 pages

DEP GCMS unknown compounds report, Mar 2002

Machine-extracted title · confidence 95%

GCMS analysis report dated March 6, 2002, listing other unknown compounds and surrogate recovery data for a different sample.

NYC-WTC_000003753–000003761

Folder label: “GCMS X 1/25/02 A 2/26/02

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Scanned page image, NYC-WTC_000003758
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C : \HPCHEM\ DATAFEB 502\1800.D Vial: 26 . Acq' On : 26 Feb 2002 2:33 pm Operator: Sample : gc/ms scan 1/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.193 339 343 354 rBV 8487 21539 1.06% 0.213% 2 12.315 787 792 808 rVB 590244 1449448 71.09% 14.309% 3 15.960 1183 1189 1206 rBV 877702 1919591 94.14% 18.950% 4 21.266 1761 1767 1782 rBV 955286 2038979 100.00% 20.128% 5 25.718 2245 2252 2264 rBV2 868713 1909871 93.67% 18.854%

6 30.795 2800 2805 2810 rBV 102916 206299 10.12% 2.037% 7 33.779 3123 3130 3149 rBV2 602982 1418714 69.58% 14.005% 8 33.990 3149 3153 3163 rVB2 11006 24659 1.21% 0.243% 9 38.057 3587 3596 3614 rBV3 361154 1140860 55.95% 11.262%

Sum of corrected areas: 10129960

1800.D GCMS0208.M Thu Feb 28 11:49:53 2002

NYC-WTC_000003758

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NYC-WTC_000003758Source: NYC Law Department, mirrored locally

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