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GCMS analysis results for sample AE01465, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01465 conducted on March 6, 2002.

NYC-WTC_000003618–000003627

Folder label: “GCMS X 1/23/02 A 2/22/02

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Scanned page image, NYC-WTC_000003626
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\1465.D Vial: 20 Acq On : 22 Feb 2002 10:47 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Propanol, 1-(2-methoxypropox Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.26 0.40 ug/1 27311 1,4-Dichlorobenzene-d4 12.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

(1 2 -PropanolDi - (2-methoxypropoxy) - 148 C7H1603 013429-07-7 83 2 2-Propanol , 1-[1-methyl-2-(2-propen 174 C9H18O3 055956-25-7 43 3 Propanoic acid, 2-hydroxy-2-methyl- 118 C5H10O3 002110-78-3 40 4 Butanoic acid, 2-hydroxy- 104 C4H803 000565-70-8 9 Abundance............................. Scan'786 (12.262 min): 1465.D (-) m/ z 59.05 100.00%

_A 59

5000

45 T 12.00 12.20 12.40 12.60 ....................... 1 111 1 1' r r 1 'i'''..IIIIt 111 .1. 73 84 194 m/z 44.95 17.06% m/z~> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #9233: 2-Propanol, 1-(2-methoxypropoxy)- 59

5000 A . ............... 12.00 12.20 12.40 12.60 31 45 m/z 43.05 11.54% 73 104 I in 1 Hi ' l i 1 ‘ I ' ' ‘ ' I ' ' 1 ' 1 1 ‘ f 1 T ‘ * I ' 1 ' 130 ' ‘ I ' 1 ‘ ' I ' * ' ' I 1 ' 1 ' I • ' 1 ' l ' ' ' I ' * m/z-> 10 20 30__ 40 50 60 70 80 90 100 110 120 130 Abundance / 6166. 2-Propu ,, i tmetny!-2-2-prpenylo~ettoxyi- 59 '

2700 12.20 12.40 12.60 5000 9.82% 103 31 45 130 73 85 117 1’1,1/"/2/111/0/1/110*1—/——/—B/1/0/*//1/0/0//00-u—nuu—OO— T m/z-> 10 20 30__ 40__ 50... 60 __ 70 80 ___ 90 100 110 120 130 Abundance #3494: Propanoic acid, 2-hydroxy-2-methyl-, methyl ester 14 ■ ■ $ 12.00 12.20 12.40 12.60 9.64% 5000 31 15 45 , 73 85 103 118 TT I ' ' ' ' I ‘ ' 1 1 I 1 11 1 I ' 1 1 1 I1'1 ' 1 I ' 1 1 1 1 1 1 1 1 1 1 1 ■ * । 1 1 1 * i * 1 1 * i ■ ■ ’ I’’ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 12.00 12.20 12.40 12.60

1465.D GCMS0208.M Tue Feb 26 15:07:04 2002 Page 2

NYC-WTC_000003626

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NYC-WTC_000003626Source: NYC Law Department, mirrored locally

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