NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
ata File : C:\HPCHEM\l\DATA\FEB2102\LBA.D Vial: 16
Acq On : 22 Feb 2002 6:50 am Operator:
Sample : gc/ms scan 1/22 Inst : GC/MS 209
. Mise : Multiplr: 1.00
/ MS Integration Params: GOOFY.P
/ Quant Time: Feb 26 12:37 2002 Quant Results File: GCMS0208.RES
/ Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Thu Feb 21 16:13:52 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 12.33 152 225704 20.00 ug/1 -0.02
10) Naphthalene-d8 15.97 136 862981 20.00 ug/1 -0.02
17) Acenaphthene-diO 21.29 164 457993 20.00 ug/1 -0.02
29) Phenanthrene-diO 25.73 188 634809 20.00 ug/1 -0.03
38) Chrysene-dl2 33.80 240 388030 20.00 ug/1 -0.04
44) Perylene-dl2 38.07 264 243012 20.00 ug/1 -0.05
System Monitoring Compounds
37) 2,4-DDD 30.81 235 36078 4.91 ug/mL 0.31
Spiked Amount 5.000 Recovery = 98.20%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.98 74 344 N.D.
3) bis(2-Chloroethyl)ether 11.73 93 442 N.D.
4) 1,3-Dichlorobenzene 12.23 146 472 N.D.
5) 1,4-Dichlorobenzene 12.37 146 453 N.D.
6) 1,2-Dichlorobenzene 12.90 146 494 N.D.
7) 2,2'-oxybi s(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 14.02 77 367 N.D.
12) Isophorone 14.68 82 1093 N.D.
13) bis(2-Chloroethoxy)methane 15.34 93 628 N.D.
14) 1,2,4-Trichlorobenzene 15.85 180 415 N.D.
15) Naphthalene 16.03 128 2375 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 19.54 162 993 N.D.
20) Dimethylphthalate 20.62 163 1140 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 20.81 152 1423 N.D.
23) Acenaphthene 21.38 153 998 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 22.76 149 1501 N.D.
26) 4-Chlorophenyl-phenylether 22.92 204 579 N.D.
27) Fluorene 22.90 166 1215 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
BA.D GCMS0208.M Tue Feb 26 12:39:34 2002 Page 1
NYC-WTC_00000357 8
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