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VOCs GC/MS lab blank results, Jan 16 2002

Machine-extracted title · confidence 95%

Gas chromatography mass spectrometry analysis report for a laboratory blank testing volatile organic compounds on January 16, 2002.

NYC-WTC_000003343–000003381

Folder label: “524 1/22/02”

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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\02JAN16\1042.D Vial: 15 Acq On : 17 Jan 2002 1:44 am Operator: 201-wb -~ Sample : nyc Inst : GC/MS Ins Misc Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Feb 5 13:01 2002 Quant Results File: HP010702.RES

Quant Method : C:\HPCHEM\1\METHODS\HP010702.M (RTE Integrator) -- Title : VOCs BY EPA METHOD 524 Last Update : Fri Jan 25 14:13:49 2002 Response via : Initial Calibration DataAcq Meth : HP010702

Internal Standards R.T. Qlon Response Conc Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.12 114 214422 5.00 ug/L -0.05 24) CHLOROBENZENE-D5 21.78 117 307013 5.00 ug/L -0.07 52) 1,4-DICHLOROBENZENE-D4 26.95 152 219746 5.00 ug/L -0.07

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.35 65 240008 8.62 ug/L -0.07 -- Spiked Amount 5.000 Recovery = 172.40% 3) 4-BROMOFLUOROBENZENE 24.36 174 130502 8.98 ug/L -0.07 Spiked Amount 5.000 Recovery = 179.60% 25) TOLUENE-D8 18.47 98 331943 4.06 ug/L -0.07 Spiked Amount 5.000 Recovery = 81.20%

Target Compounds Qvalue 5) CHLOROMETHANE 5.69 50 5507 0.53 ug/L 90 7) BROMOMETHANE 6.80 94 1270 0.19 ug/L 53 8) CHLOROETHANE 6.78 64 1414 0.23 ug/L 90 10) Isopropyl Alcohol 7.94 45 2770 11.95 ug/L 96 11) 1,1,2-Trichloro-1,2,2-trif 8.12 101 1872 0.17 ug/L 97 12) ACETONE 8.27 43 17518 6.30 ug/L 91 18) 2-BUTANONE (MEK) 12.05 43 9044 2.21 ug/L 65 46) 2-HEXANONE 19.20 43 1526 0.22 ug/L 66

------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 1042.D HP010702.M Tue Feb 05 13:02:05 2002 Page 1

NYC-WTC 000003372

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NYC-WTC_000003372Source: NYC Law Department, mirrored locally

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VOCs GC/MS lab blank results, Jan 11 2002 · Box DEP Box 04

NYC-WTC_000003326

Gas chromatography mass spectrometry analysis report for a laboratory blank testing volatile organic compounds on January 11, 2002.

6 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995

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