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← Document results/DEP Box 04/524 1/22/02
Document / 77 pages

VOCs GC/MS analysis results, Jan 22-23 2002

Machine-extracted title · confidence 90%

Laboratory report showing volatile organic compound analysis results for sample AE01036 processed on January 22 and 23, 2002.

NYC-WTC_000003249–000003325

Folder label: “524 1/22/02”

Page image
Scanned page image, NYC-WTC_000003254
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\02JAN22\0122B2.D Vial: 2 Acq On : 22 Jan 2002 9:18 am Operator: Sample : lab blank 2 Inst : 210 Misc : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP010802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2H-Thiopyran-3(6H)-one Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 18.33 0.04 ug/L 12604 1,4-DIFLUOROBENZENE 17.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------------------------------------------------------------- 1 2H-Thiopyran-3(6H)-one 114 C5H6OS 029431-30-9 4 2 3-Cyclobutene-1,2-dione, 3,4-dihydr 114 C4H2O4 002892-51-5 4 3 Ethanol, 2-chloro-, propanoate 136 C5H9C1O2 001487-40-7 4 4 Ethene, (2-chloroethoxy)- 106 C4H7C1O 000110-75-8 4 aance an 1311 (18.329 min): 0122B2.D (-) m/ Z 113. y s l U U. U U 14

5000 40

50 62 81 18.00 18.20 18.40 18.60 75 m Z 39. 5 4b.24 > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 dance #2850: 2H-Thlopyran-3(6H)-one

5000 85 114 18.00 18.20 18.40 18.60 6 m Z 1.O5 14.94%

> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 dance #2826: 3-Cyclobutene-1,2-dione, 3,4-dihydroxy- 58

18.00 18.20 18.40 18.60 m z 61.95 14.62 5000 114

86 17 40 68 > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 dance #6383: Ethanol, 2-chioro-, propanoate ) 'P 63 18.00 18.20 18.40 18.60

5000

91 45 99 108 136 > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 18.00 18.20 18.40 18.60

0122B2.D HP010802.M Fri Jan 25 11:51:46 2002 Page 1

NYC-WTC 000003254

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NYC-WTC_000003254Source: NYC Law Department, mirrored locally

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