WTC sample cover sheet, Dec 19 2001

NYC 9111 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\O1dec20\l220CIO.D Acq On Vial: 8 : 20 Dec 2001 10:08 am Operator: 206-BH Sample : cal 10 Inst : GC/MS Ins Misc MS Integration Params: LSCINT.P Multiplr: 1.00 Quant Time: Dec 20 10:46 2001 Quant Results File: HP121001.RES Quant Method : C:\HPCHEM\1\METHODS\HP121001.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu Dec 20 09:38:26 2001 Response via : Initial Calibration DataAcq Meth : HP121001

Internal Standards R.T. Qlon Response Conc Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 14.44 114 687991 5.00 ug/L 0.08 22) CHLOROBENZENE-D5 21.03 117 665094 5.00 ug/L 0.07 50) 1,4-DIFHLOROBENZENE-D4 26.21 152 459362 5.00 ug/L 0.10 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 13.65 65 266983 5.89 ug/L 0.07 Spiked Amount 5.000 Recovery = 117.80% 3) 4-BROMOFLUOROBENZENE 23.62 174 279497 5.29 ug/L 0.08 Spiked Amount 5.000 Recovery = 105.800 . 23) TOLUENE-D8 17.76 98 879471 4.99 ug/L 0.08 Spiked Amount 5.000 Recovery = 99.800 Target Compounds 4) DICHLORODIFLUOROMETHANE Qvalue 4.48 85 320026 14.25 ug/L 100 5) CHLOROMETHANE 5.00 50 256436 18.37 ug/L 99 6) VINYL CHLORIDE 5.17 62 274094 19.74 ug/L 95 7) BROMOMETHANE 6.09 94 210988 17.38 ug/L 100 8) CHLOROETHANE 6.21 64 165609 17.40 ug/L 97 9) TRICHLOROFLUOROMETHANE 6.75 101 454597 15.09 ug/L 99 10) ACETONE 7.69 43 52717 11.42 ug/L 94 11) 1,1-DICHLOROETHENE 8.03 61 359302 9.19 ug/L 94 12) METHYLENE CHLORIDE 9.00 49 395754 10.44 ug/L 92 13) METHYL TERT BUTYL ETHER 9.29 73 448418 8.97 ug/L 100 14) TRANS-1,2-DICHLOROETHENE 9.65 61 402828 9.50 ug/L 92 15) 1,1-DICHLOROETHANE 10.54 63 516231 9.76 ug/L 98 16) 2-BUTANONE (MEK) 11.35 43 84879 10.41 ug/L 97 17) 2,2-DICHLOROPROPANE 11.73 77 450778 10.34 ug/L 100 18) CIS-1,2-DICHLOROETHENE 11.81 96 277097 9.35 ug/L 93 19) CHLOROFORM 12.16 83 550610 10.91 ug/L 98 20) BROMOCHLOROMETHANE 12.53 49 258138 10.78 ug/L 94 21) 1,2-DICHLOROETHANE 13.86 62 360141 10.60 ug/L 98 24) 1,1,1-TRICHLOROETHANE 13.02 97 441467 10.81 ug/L 98 25) 1,1-DICHLOROPROPENE 13.36 75 414141 10.27 ug/L 99 26) CARBON TETRACHLORIDE 13.62 117 394161 11.34 ug/L 98 27) BENZENE 13.96 78 1118203 9.54 ug/L 98 28) TRICHLOROETHENE 15.22 95 310800 9.90 ug/L 98 29) 1,2-DICHLOROPROPANE 15.58 63 312837 9.58 ug/L 99 30) DIBROMOMETHANE 16.23 174 111265 9.58 ug/L 97 31) BROMODICHLOROMETHANE 16.09 83 416573 11.08 ug/L 100 32) 2-CHLOROETHYL VINYL ETHER 16.58 63 107131 8.84 ug/L 94 33) Methyl iso-butyl ketone 16.65 58 57793 9.27 ug/L 95 --------------------------------------------- (#) = qualifier out of range (m) = manual integration 1220C10.D HP121001.M Thu Dec 20 10:46:49 2001 Page 1

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