Reference recovery analysis for Site 524, Nov 2001

NYC 9/11 Public Portal Document

• Quantitation Report (Not Reviewed) • Data File : C:\HPCHEM\1\DATA\01nov8\1108R40.D Vial: 7 Acq On 8 Nov 2001 2:02 pm Operator: Sample : ref 40 Inst : GC/MS Ins Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Nov 8 14:41 2001 Quant Results File: HP110101.RES

Quant Method : C:\HPCHEM\1\METHODS\HP110101.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri Nov 02 15:17:46 2001 Response via : Initial Calibration DataAcq Meth : HP110101

Compound R.T. Qlon Response Conc Unit Qvalue ------------------------------------------------------------------------- 34) CIS-1,3-DICHLOROPROPENE 17.18 75 1920605 41.49 ug/L 99 35) TOLUENE 17.93 91 5840407 42.35 ug/L 100 36) TRANS-I,3-DICHLOROPROPENE 18.20 75 1355186 39.57 ug/L 99 37) 1,1,2-TRICHLOROETHANE 18.60 97 667607 38.65 ug/L 98 38) TETRACHLOROETHENE 19.36 166 1179782 51.14 ug/L 99 39) 1,3-DICHLOROPROPANE 19.11 76 1385944 39.22 ug/L 99 40) DIBROMOCHLOROMETHANE 19.79 129 733765 44.16 ug/L 100 41) 1,2-DIBROMOETHANE 20.23 107 614111 41.19 ug/L 99 42) CHLOROBENZENE 21.12 112 3708791 44.64 ug/L 98 43) 1,1,1,2-TETRACHLOROETHANE 21.17 131 1072661 46.08 99 ug/L

44) 2-HEXANONE 18.49 43 435409 44.63 ug/L 97 45) ETHYLBENZENE 21.17 91 7263580 44.36 ug/L 98 46) P & M-XYLENE 21.32 106 5163255 90.05 98 ug/L

47) O-XYLENE 22.29 91 5614044 44.20 ug/L 100 48) STYRENE 22.34 104 3970978 43.76 ug/L 99 49) 1,1,2,2-TETRACHLOROETHANE 23.37 83 739893. 41.56 100 ug/L

51) BROMOFORM 23.18 173 303381 51.34 99 ug/L

52) ISOPROPYLBENZENE 23.01 105 6645503 44.31 99 ug/L

53) 1,2,3-TRICHLOROPROPANE 23.69 110 181504 38.47 94 ug/L

54) N-PROPYLBENZENE 23.88 91 8995280 44.18 99 ug/L

55) BROMOBENZENE 24.12 156 1125856 42.74 89' ug/L

56) 1,3,5-TRIMETHYLBENZENE 24.20 105 5391450 42.10 100 ug/L

57) 2-CHLOROTOLUENE 24.35 91 5102094 41.95 ug/L

99 58) 4-CHLOROTOLUENE 24.42 91 4979118 41.73 100 - ug/L

.5-9-) TERT-BUTYLBENZENE 24.99- 134 1193928 46.32-ug/L 10-01- 60) 1,2,4-TRIMETHYLBENZENE 25.09 105 5489863 40.97 ug/L

99 61) SEC-BUTYLBENZENE 25.45 105 7828138 44.16 ug/L 100 62) P-ISOPROPYLTOLUENE 25.70 119 5849376 42.37 ug/L 100 63) 1,3-DICHLOROBENZENE 26.04 146 2526287 43.45 ug/L

99 64) 1,4-DICHLOROBENZENE 26.26 146 2492023 43.46 ug/L

99 65) N-BUTYLBENZENE 26.59 91 6297673 40.83 ug/L

99- - 66) 1,2-DICHLOROBENZENE 27.10 146 2046754 42.88 ug/L

99 67) 1,2-DIBROMO-3-CHLOROPROPAN 28.75 157 89024 43.42 ug/L

100 $8) NITROBENZENE --

28.94 - 77 1237394 1366.26 ug/L 95- 69) 1,2,4-TRICHLOROBENZENE 30.69 180 1106781 43.78 ug/L

99 70) HEXACHLOROBUTADIENE 30.93 225 650812 54.70 ug/L 98 71) NAPHTHALENE 31.36 128 1290234 33.67 ug/L 100 . 72) 1,2,3-TRICHLOROBENZENE 31.92 180 762339 41.18- ug/L 99

------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 1108R40.D HP110101.M Thu Nov 08 14:41:40 2001 Page 2

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