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VOC duplicate analysis results, sample AD24356, Oct 10 2001

Machine-extracted title · confidence 100%

DEP duplicate calculation report for sample AD24356 analyzing volatile organic compounds on October 10, 2001.

NYC-WTC_000000825–000000830

Folder label: “524 up to 11/7/01

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\0loctl5\24356D.D Vial: 5 Acq On : 15 Oct 2001 3:45 pm Operator: Sample : dup Inst : GC/MS Ins Misc Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Oct 15 16:24 2001 Quant Results File: HP092601.RES

Quant Method : C:\HPCHEM\1\METHODS\HP092601.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Wed Sep 26 08:36:04 2001 Response via : Initial Calibration DataAcq Meth : HP092601

Internal Standards R.T. Qlon Response Conc Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 14.46 114 1012302 5.00 ug/L -0.10 22) CHLOROBENZENE-D5 21.05 117 870939 5.00 ug/L -0.10 50) 1,4-DICHLOROBENZENE-D4 26.21 152 368354 5.00'ug/L -0.10

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 13.67 65 208804 4.60 ug/L -0.10 Spiked Amount 5.000 Recovery = 92.00% 3) 4-BROMOFLUOROBENZENE 23.62 174 260004 3.49 ug/L -0.12 Spiked Amount 5.000 Recovery = 69.80% 23) TOLUENE-D8 17.78 98 1236340 5.37 ug/L -0.10 Spiked Amount 5.000 Recovery = 107.40%

Target Compounds Qvalue 10) ACETONE 7.71 43 12188 3.21 ug/L 92 16) 2-BUTANONE (MEK) 11.39 43 5486 0.74 ug/L 96 19) CHLOROFORM 2? 12.16 83 1958419 27.40 ug/L 99 31) BROMODICHLOROMETHANE e-( 16.09 83 276409 6.44 ug/L 100 35) TOLUENE 17.95 91 33853 ..8--19--t -f! 96 40) DIBROMOCHLOROMETHANE /.3 19.81 129 33710 1.33 ug/L. 97 51) BROMOFORM .V( 23.20 173 4067 0.41 ug/L 92

------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 24356D.D HP092601.M Mon Oct 15 16:24:28 2001 Page 1

NYC-WTC 000000829

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NYC-WTC_000000829Source: NYC Law Department, mirrored locally

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