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Volatile organic compounds analysis, sample AD26320, Oct 2001

Machine-extracted title · confidence 85%

DEP laboratory analysis of sample AD26320 for volatile organic compounds including dichloroethane, MEK, and chlorinated hydrocarbons, completed October 29-30, 2001.

NYC-WTC_000000746–000000749

Folder label: “524 up to 11/7/01

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File . C:\HPCHEM\1\DATA\01OCT29\1029B1.D Vial: 1 Acq On : 29 Oct 2001 10:29 am Operator: Sample : lb Inst : GC/MS Ins Misc Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Oct 29 11:22 2001 Quant Results File: HP102901.RES

Quant Method : C:\HPCHEM\1\METHODS\HP102901.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Mon Oct 29 11:21:05 2001 Response via : Initial Calibration DataAcq Meth : HP102901

Internal Standards R.T. Qlon Response Conc Units Dev(Min) ------------------------------------------------------------------------- 1) 1,4-DIFLUOROBENZENE 14.34 114 1051907 5.00 ug/L -0.22 22) CHLOROBENZENE-D5 20.93 117 1073677 5.00 ug/L -0.22 50) 1,4-DICHLOROBENZENE-D4 26.09 152 530524 5.00 ug/L -0.22

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 13.55 65 301567 4.75 ug/L -0.22 Spiked Amount 5.000 Recovery = 95.00% , 3) 4-BROMOFLUOROBENZENE 23.50 174 372521 5.04 ug/L -0.24 Spiked Amount 5.000 Recovery = 100.80%/ 23) TOLUENE-D8 17.66 98 1414715 4.95 ug/L -0,22 Spiked Amount 5.000 Recovery = 99.000./

Target Compounds Qvalue 16) 2-BUTANONE (MEK) 11.29 43 4351 0.38 ug/L 53 19) CHLOROFORM 12.05 83 30951 0.42 ug/L 100 66) 1,2-DICHLOROBENZENE 27.01 146 10730 0.13 ug/L 93 67) 1,2-DIBROMO-3-CHLOROPROPAN 28.67 157 1162 0.29 ug/L 97 CCU 69) 1,2,4-TRICHLOROBENZENE 30.59 180 39737 -0.71 ug/L 99 70) HEXACHLOROBUTADIENE 30.83 225 19907 ' 0.65 ug/L 95 71) NAPHTHALENE 31.25 128 90482 \1.18 ug/L 99 72) 1,2,3-TRICHLOROBENZENE 31.80 180 82561 ~-1.74 ug/L 95

------------------------------------------------------------------------- (##) = qualifier out of range (m) = manual integration 1029B1.D HP092601.M Tue Nov 13 11:08:57 2001 Page 1

NYC-WTC 000000748

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NYC-WTC_000000748Source: NYC Law Department, mirrored locally

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