DEP form with redacted names, Jan 24 2002

NYC 9/11 Public Portal Document Luai1l.iLau-Lui1 kceyuLL I1JuL ke. _Leneu)

Data File : C:\HPCHEM\1\DATA\02JAN24\0124C10D.D Vial: 13 Acq On : 25 Jan 2002 2:42 am Operator: 201-wb Sample : cal 10 Inst : GC/MS Ins Misc : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Jan 25 14:14 2002 Quant Results File: HP010702.RES

Quant Method : C:\HPCHEM\1\METHODS\HP010702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri Jan 25 14:13:49 2002 Response via : Initial Calibration DataAcq Meth : HP010702

Internal Standards R.T. Qlon Response Conc Units Dev(Min) ------------------------------------------------------------------------- 1) 1,4-DIFLUOROBENZENE 15.17 114 929219 5.00 ug/L 0.00 24) CHLOROBENZENE-D5 21.83 117 760073 5.00 ug/L -0.02 52) 1,4-DICHLOROBENZENE-D4 27.00 152 365248 5.00 ug/L -0.02

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.41 65 609467 5.05 ug/L -0.02 Spiked Amount 5.000 Recovery = 101.00% 3) 4-BROMOFLUOROBENZENE 24.41 174 287928 4.57 ug/L -0.02 Spiked Amount 5.000 Recovery = 91.40% 25) TOLUENE-D8 18.52 98 1111616 5.49 ug/L -0.02 Spiked Amount 5.000 Recovery = 109.80%

Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.90 85 676568 16.61 ug/L 99 5) CHLOROMETHANE 5.54 50 547799 12.11 ug/L 93 6) VINYL CHLORIDE 5.62 62 470262 12.59 ug/L 97 7) BROMOMETHANE 6.65 94 376174 12.73 ug/L 92 8) CHLOROETHANE 6.78 64 304003 11.62 ug/L 99 9) TRICHLOROFLUOROMETHANE 7.33 101 910653 12.35 ug/L 97 10) Isopropyl Alcohol 7.98 45 2236 2.23 ug/L 81 11) 1,1,2-Trichloro-1,2,2-trif 8.24 101 427753 8.77 ug/L 98 12) ACETONE 8.33 43 116451 9.66 ug/L 97 13) 1,1-DICHLOROETHENE 8.67 61 644818 8.73 ug/L 99 14) METHYLENE CHLORIDE 9.68 49 776490 9.08 ug/L 99 15) METHYL TERT BUTYL ETHER 9.98 73 418641 8.38 ug/L 99 16) TRANS-1,2-DICHLOROETHENE 10.35 61 694786 9.50 ug/L 98 17) 1,1-DICHLOROETHANE 11.23 63 759203 9.45 ug/L 99 18) 2-BUTANONE (MEK) 12.07 43 159901 10.10 ug/L 97 19) 2,2-DICHLOROPROPANE 12.45 77 407910 7.26 ug/L 100 20) CIS-1,2-DICHLOROETHENE 12.54 96 389753 9.56 ug/L 98 21) CHLOROFORM 12.89 83 851026 9.27 ug/L 97 22) BROMOCHLOROMETHANE 13.26 49 414122 8.94 ug/L 92 23) 1,2-DICHLOROETHANE 14.60 62 691399 9.07 ug/L 96 26) 1,1,1-TRICHLOROETHANE 13.78 97 686089 9.90 ug/L 96 27) 1,1-DICHLOROPROPENE 14.11 75 549592 10.23 ug/L 98 28) CARBON TETRACHLORIDE 14.37 117 690267 9.91 ug/L 98 29) BENZENE 14.70 78 1487483 10.68 ug/L 98 30) TRICHLOROETHENE 15.97 95 424012 9.92 ug/L 98 31) 1,2-DICHLOROPROPANE 16.34 63 402158 10.05 ug/L 99 32) DIBROMOMETHANE 17.00 174 164255 9.29 ug/L 94 33) BROMODICHLOROMETHANE 16.85 83 564813 9.55 ug/L 99 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 0124C10D.D HP010702.M Fri Jan 25 14:15:09 2002 Page 1

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